烷基苯磺酸盐纯化工艺研究

doi:10.3969/j.issn.1006-396X.2017.04.001

石油化工高等学校学报 ›› 2017, Vol. 30 ›› Issue (4): 1-5.DOI: 10.3969/j.issn.1006-396X.2017.04.001

烷基苯磺酸盐纯化工艺研究

王帅¹，郭兰磊²，祝仰文²，潘斌林²，王红艳²，郭勇¹

1. 中国科学院兰州化学物理研究所中国科学院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室，甘肃兰州 730000

2. 中国石化胜利油田勘探开发研究院，山东东营 257015

收稿日期:2017-01-18 修回日期:2017-04-20 出版日期:2017-08-29 发布日期:2017-08-29
作者简介:王帅(1979-),男,博士,研究员,主要从事油田化学分离、分析方面研究;E-mail:shuaiw@licp.cas.cn。
基金资助:
国家科技重大专项“胜利油田特高含水期提高采收率技术(二期)”(2016ZX05011-003-006)

Purification Process of Alkylbenzene Sulfonates

1.CAS Key Laboratory of Chemistry of Northwestern Plant Resources and Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences(CAS), Lanzhou Gansu 730000, China;

2. SINOPEC Research Institute of Exploration & Development, Shengli Oilfield, Dongying Shandong 257015, China

Received:2017-01-18 Revised:2017-04-20 Published:2017-08-29 Online:2017-08-29

摘要/Abstract

摘要：

结合同步监控技术，采用液液萃取法对烷基苯磺酸盐样品中的烷基苯磺酸盐活性物进行分离纯化。结果表明，优化后的纯化工艺可以获得纯度较高、结果更为准确的烷基苯磺酸盐活性物组分，样品中其它共存组分如未磺化油、无机盐等中残留的烷基苯磺酸盐活性物的量小于总活性物量的1%；采用优化后的纯化工艺获得的烷基苯磺酸盐活性物质量分数较常规纯化工艺有明显增加，从39%左右增加至48%以上。

关键词: 烷基苯磺酸盐, 活性物, 纯化, 质量分数

Abstract:

Combined with synchronized monitoring techniques, the active constituent in the sample of alkylbenzene sulfonates was separated and purified by liquidliquid extraction method. The results showed that the active constituent with higher purity can be obtained and the content data were more accurate adopting the present optimized purification process. Meanwhile, the residual content of active constituent of alkylbenzene sulfonates in the coexist constituents, such as unsulfonated oil, inorganic salts etc. was less than 1% of the total active amount. The content of active constituent of alkylbenzene sulfonates increased from about 39% to 48% compared to the purification process that is usually used previously.

Key words: Alkylbenzene sulfonate, Active constituent;, Purification;, Content

王帅，郭兰磊，祝仰文等. 烷基苯磺酸盐纯化工艺研究[J]. 石油化工高等学校学报, 2017, 30(4): 1-5.

Wang Shuai, Guo Lanlei, Zhu Yangwen,et al. Purification Process of Alkylbenzene Sulfonates[J]. Journal of Petrochemical Universities, 2017, 30(4): 1-5.

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烷基苯磺酸盐纯化工艺研究

Purification Process of Alkylbenzene Sulfonates

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