深冷条件下多重旋转碾压超细晶铜的组织与磨损性能

doi:10.12422/j.issn.1672-6952.2024.02.008

辽宁石油化工大学学报 ›› 2024, Vol. 44 ›› Issue (2): 50-54.DOI: 10.12422/j.issn.1672-6952.2024.02.008

深冷条件下多重旋转碾压超细晶铜的组织与磨损性能

周华¹(), 贾南¹, 陆亚轩¹, 孟祥晨², 黄永宪²()

^1.河钢工业技术服务有限公司，河北廊坊 065000
^2.先进焊接与连接国家重点实验室，黑龙江哈尔滨 150001

收稿日期:2023-06-09 修回日期:2023-08-21 出版日期:2024-04-25 发布日期:2024-04-24
通讯作者: 黄永宪
作者简介:周华（1987⁃），男，工程师，从事结晶器修复与增材制造方面的研究；E⁃mail：zhouhuau01@hbisco.com。
基金资助:
国家自然科学基金项目(52175301);航空发动机及燃气轮机专项资助项目（J2019?Ⅶ?0012?0154）;中国博士后科研基金项目(2021T140151)

Microstructures and Wear Properties of Ultrafine⁃Grained Cu via Multiple Rotational Rolling under Deep Cooling Condition

Hua ZHOU¹(), Nan JIA¹, Yaxuan LU¹, Xiangchen MENG², Yongxian HUANG²()

^1.HBIS Industrial Technical Service Co. ，Ltd. ，Langfang Hebei 065000，China
^2.State Key Laboratory of Advanced Welding and Joining，Harbin Heilongjiang 150001，China

Received:2023-06-09 Revised:2023-08-21 Published:2024-04-25 Online:2024-04-24
Contact: Yongxian HUANG

摘要/Abstract

摘要：

通过碾压式搅拌头在深冷条件下对铜板进行多重旋转碾压，采用超景深显微镜、光学显微镜、摩擦磨损仪对碾压后样品的表面形貌、组织和性能进行了分析。结果表明，在深冷条件下多重旋转碾压后，样品表面成形良好，表层出现明显的超细晶区；在转速为50 r/min时，超细晶成形机制为晶粒的剪切破碎；在转速为500 r/min时，晶粒细化机制为动态再结晶和强制冷却抑制再结晶晶粒的长大；在深冷条件下多重旋转碾压制备的超细晶层可提高材料的耐磨性。

关键词: 多重旋转碾压, 超细晶, 再结晶机制, 磨损性能

Abstract:

The Cu plate was fabricated by a novel grinding tool via multiple rotational grinding under deep cooling condition. The surface morphology, microstructures and properties of the grinding zone were analyzed via super depth of field microscope, optical microscope, friction and wear test, respectively. The results show that well surface formation and ultrafine grains were obtained after multiple rotational grinding under deep cooling condition. Combined with the temperature distribution simulation, the main grain refinement mechanism of 50 r/min is the breaking and split of the grain. The grain refinement mechanism at 500 r/min is dynamic recrystallization and forced cooling to inhibit the growth of recrystallized grains. Microhardness tests and wear tests showed that the ultrafine?grained zone prepared by multiple rotational grinding under deep cooling condition could improve the wear resistance of the materials.

Key words: Multiple rotational grinding, Ultrafine grain, Grain refinement mechanism, Wear properties

中图分类号:

TG441.8

周华, 贾南, 陆亚轩, 孟祥晨, 黄永宪. 深冷条件下多重旋转碾压超细晶铜的组织与磨损性能[J]. 辽宁石油化工大学学报, 2024, 44(2): 50-54.

Hua ZHOU, Nan JIA, Yaxuan LU, Xiangchen MENG, Yongxian HUANG. Microstructures and Wear Properties of Ultrafine⁃Grained Cu via Multiple Rotational Rolling under Deep Cooling Condition[J]. Journal of Liaoning Petrochemical University, 2024, 44(2): 50-54.

图/表 8

表1 铜板的化学组成

Table 1 Chemical composition of Cu plate

组分	质量分数/%	组分	质量分数/%
Sb	≤0.002	Sn	≤0.002
As	≤0.002	S	≤0.005
Fe	≤0.005	Zn	≤0.005
Ni	≤0.002	Cu+Ag	余量
Pb	≤0.003

图1 多重旋转碾压头（a）碾压头组装图（b）碾压头拆分图

Fig.1 Multiple rotational grinding tool

图2 深冷条件下多重旋转碾压铜板表面的宏观形貌

Fig.2 Surface morphologies of Cu plate via multiple rotational grinding under deep cooling condition

图3 不同条件下碾压区的表面三维形貌

Fig.3 Surface three?dimensional morphology of the grinding zone under different conditions

图4 碾压区横截面微观组织

Fig.4 Cross?sectional microstructure of the grinding zone

图5 晶粒细化机制

Fig.5 Grain refinement mechanism

图6 不同条件下的温度场分布云图

Fig.6 Cloud maps of temperature field distribution under different conditions

图7 碾压区摩擦磨损结果注：蓝色、红色、绿色、黑色的点分别为母材及其在下压量为0.1、0.2、0.3 mm的条件下测得的原始数据；对应的线为对原始数据进行拟合得到的曲线。

Fig.7 Wear test results of the grinding zone

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深冷条件下多重旋转碾压超细晶铜的组织与磨损性能

Microstructures and Wear Properties of Ultrafine⁃Grained Cu via Multiple Rotational Rolling under Deep Cooling Condition

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