Salt Cosolvent-Combustion Rapidly Synthesized Small-Size Rod Zinc Oxide

doi:10.3969/j.issn.1006-396X.2012.05.005

Journal of Petrochemical Universities ›› 2012, Vol. 25 ›› Issue (5): 18-21.DOI: 10.3969/j.issn.1006-396X.2012.05.005

Previous Articles Next Articles

Salt Cosolvent-Combustion Rapidly Synthesized Small-Size Rod Zinc Oxide

1. School of Chemistry & Material, Liaoning Shihua University, Fushun Liaoning 113001, P.R.China； 2.School of Petrochemical Engineering, Liaoning Shihua University, Fushun Liaoning 113001, P.R.China; 3.CNPC Fushun Chemical Plastics Plant, Fushun Liaoning 113005, P.R.China

Received:2012-06-01 Published:2012-10-25 Online:2012-10-25

盐助溶燃烧法快速合成小粒径棒状氧化锌

李秀萍¹,赵荣祥²,刘春生¹,高霄汉¹,冯锦烨³

1.辽宁石油化工大学化学与材料科学学院,辽宁抚顺113001;2.辽宁石油化工大学石油化工学院,辽宁抚顺113001;3.中国石油抚顺石化分公司抚顺化工塑料厂,辽宁抚顺113005

作者简介:李秀萍（１９７５－），辽宁康平县，讲师，在读博士
基金资助:
国家青年基金项目（２１００３０６９）

Abstract

Abstract: With zinc nitrate as the oxidant and ascorbic acid as reducing agent and a new burners, combustion rapidly synthesized milky and rod zinc oxide. The burning agent dose, calcined or not, calcination temperature, adding cosolvent or not were inspected. The experiment show ratio of ascorbic acid and zinc [KG*4]nitrate [KG*4]is [KG*4]3∶1, ratio [KG*4]of [KG*4]ascorbic [KG*4]acid [KG*4]and [KG*4]cosolvent is 1∶ 0.5. Product of combustion wasnt calcined and washed, which is high purity and good crystallinity. The samples more fluffy and shorter by adding cosolvent. The sample was characterized by FTIR, XRD, UV-Vis, SEM. Zinc oxide has strong absorption in UV-Vis and IR wave band，particles size is micron, morphology is short rod.

Key words: Combustion method, Rod, Zinc oxide

摘要： 采用一种新型还原性的燃烧剂抗坏血酸与氧化性的六水合硝酸锌为原料，燃烧法合成乳白色棒状氧化锌，对燃烧剂的用量、是否煅烧和煅烧温度、是否加入助溶剂进行考察。结果表明，燃烧剂与六水合硝酸锌的物质的量之比为3∶1，六水合硝酸锌与助溶剂物质的量之比为1∶0.5，样品不经洗涤和煅烧，其纯度和结晶度较高。加入助溶剂样品更加蓬松，样品棒更短。样品经FTIR, XRD, UV-Vis, SEM表征，结果表明所制备的氧化锌在紫外和红外都有强吸收，粒径可达微米级，形貌为短的棒状。

关键词: 燃烧法 , 棒状 , 氧化锌

LI Xiu-ping,ZHAO Rong-xiang,LIU Chun-sheng,et al. Salt Cosolvent-Combustion Rapidly Synthesized Small-Size Rod Zinc Oxide[J]. Journal of Petrochemical Universities, 2012, 25(5): 18-21.

李秀萍,赵荣祥,刘春生,高霄汉,冯锦烨. 盐助溶燃烧法快速合成小粒径棒状氧化锌[J]. 石油化工高等学校学报, 2012, 25(5): 18-21.

[1]	Feifei HAN, Jianhao JIAO, Xiangchen TIAN, Ye YANG, Yucai QIN, Lijuan SONG. Effect of Sn Introduction on the Dehydrogenation Performance of Propane of Al₂O₃⁃Supported Pt⁃Based Catalysts [J]. Journal of Petrochemical Universities, 2024, 37(4): 49-56.
[2]	Nan CHEN. Experimental and Numerical Simulation Study on Shut⁃In or Adjustment of Injection Production Wells under Different Injection Production Conditions [J]. Journal of Petrochemical Universities, 2024, 37(2): 9-15.
[3]	Mengshan Liu, Chao Meng, Han Hu, Mingbo Wu. Preparation of NiMoN Catalytic Electrode Material for Hydrogen Production via Seawater Electrolysis [J]. Journal of Petrochemical Universities, 2023, 36(2): 1-9.
[4]	Yuwei Ouyang, Ming Long, Jilei Zhang, Quan Li, Liqin Gan. Law of Liquid Production in Increase in Fluvial Facies Reservoir of Bohai Q Oilfield [J]. Journal of Petrochemical Universities, 2023, 36(1): 32-39.
[5]	Yana Ju, Yalin Zhang, Ran Zhang, Shaotong Song, Lü Zhongwu, Xiaoliang Yuan, Yang Li, Pei Wu. Study on the Effect of Metal Dispersion on the Catalytic Activity of Nickel⁃Based Catalysts [J]. Journal of Petrochemical Universities, 2022, 35(5): 71-77.
[6]	Jianping Yang. Production Decline Analysis Method of Heavy Oil Thermal Recovery Based on Steam Soaking [J]. Journal of Petrochemical Universities, 2022, 35(3): 70-74.
[7]	Tian Fang, Yiyin Gao, Siyu Wang, Li Wang, Yun Guo, Yanglong Guo. Reaseching on Supported Noble Metals over Mn⁃Zr Composite Oxides for the Catalytic Combustion of Vinyl Chloride [J]. Journal of Petrochemical Universities, 2021, 34(5): 1-8.
[8]	Qi Xiong. Productivity Evaluation and Production Improvement of Offshore Low Permeability Oilfield: A Case Study of Xijiang Oilfield [J]. Journal of Petrochemical Universities, 2021, 34(5): 43-49.
[9]	Li Dai, Hongjun Yin, Hongfei Yuan, Fansong Meng. Production Decline Analysis of Vertical Well with Multi⁃Layer Network Fracturing in Tight Oil Reservoir [J]. Journal of Petrochemical Universities, 2021, 34(5): 50-55.
[10]	Xianzhong Wang. Construction and Practice of Long⁃Distance Product Oil Pipeline Management System Based on Risk Management [J]. Journal of Petrochemical Universities, 2021, 34(5): 91-96.
[11]	Zhang Dong， Sun Enhui， Yang Dongdong， Tan Jie. A New Method of Bottom⁃Water Reservoir Development Prediction Based on Data Mining [J]. Journal of Petrochemical Universities, 2021, 34(3): 84-89.
[12]	Li Zhimin， Pang Yanping， Zhang Jing， Sun Xitong， Qi Xiangdong. Study on Saling Deposition in Water Collecting Tubes of Produced Water Downward Flow Filter in Oilfield [J]. Journal of Petrochemical Universities, 2021, 34(2): 47-53.
[13]	Ma Rui1， Song Yongyi， Zhang Qingjun， Zhang Shudong， Liu Jihua， Li Xiaohui， Zhang Qingyao. Progress of Residual Marine Fuel Desulfurization Technology [J]. Journal of Petrochemical Universities, 2021, 34(1): 15-21.
[14]	Zhang Jing， Pang Yanping， Li Zhimin， Wang Zhihua. Effect of Dissolved⁃Air Flotation on Flow Field Characteristics of Produced Water in Settlement Separation Process [J]. Journal of Petrochemical Universities, 2021, 34(1): 72-79.
[15]	Wang Wei. Analysis on Influential Factors for Initial Productivity of the Network Fracturing Vertical Well in Tight Oil Reservoir [J]. Journal of Petrochemical Universities, 2020, 33(6): 37-42.

Salt Cosolvent-Combustion Rapidly Synthesized Small-Size Rod Zinc Oxide

盐助溶燃烧法快速合成小粒径棒状氧化锌

PDF

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics