Journal of Petrochemical Universities ›› 2010, Vol. 23 ›› Issue (2): 61-63.

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Research on the Preparation and Performance of Chitosan Membrane

  

  1. 1. School of Bioengineering, Xihua University, Chengdu Sichuan 610039,P.R.China; 
    2. International Affairs Department, Liaohe Petroleum Exploration Bureau, Panjin Liaoning 124010, P.R.China
  • Received:2009-01-08 Published:2010-06-25 Online:2010-06-25

壳聚糖缓释膜的制备及性能研究

蒋珍菊,孙仲,王周玉   

  1. 1 .西华大学生物工程学院, 四川成都610039 ; 2 .辽河石油勘探局国际事业部
  • 作者简介:蒋珍菊(1974 -), 女, 四川安岳县, 副教授, 博士
  • 基金资助:
    中国石油天然气集团公司中青年创新基金(部(基349));四川省重点学科建设项目资助。

Abstract:

The chitosan membrane and crosslineked were prepared by doctor-blade casting process with chitosan. The chitosan solution concentration as well as temperature capacity of glutaraldehyde crosslinked chitosan membranes have been studied. The best experimental conditions of cross-linking of chitosan film have been obtained as follows: the concentration of chitosan solution is 1%, cross linking temperature would be exceeded 70 ℃,  cross linking time must be exceeded 1 h, and to obtain the better film, the dry way would be the nature air dries or drying on the 80 ℃. The results show that chitosan membrane has the highest intensity of 9.92 MPa, the maximum ratio of  resistant elongation is 11.75%, and the film has not the acid resistance. Though the cross-linked chitosan with glutaric the highest intensity of  dialdehyde can achieve the value 96.64 MPa, the maximum ratio of  resistant elongation is 10.92%. The acid resistance of film has been enhanced greatly.
 

Key words:

摘要: 以壳聚糖为原料, 采用流延法制备了壳聚糖膜, 并与戊二醛交联所制备的膜进行了简单的性能比较,
得出实验条件为:壳聚糖质量分数为1 %的溶液, 交联温度为70 ℃以上, 交联时间1 h 以上, 自然晾干或80 ℃烘干,
成膜比较好。结果表明, 壳聚糖膜有一定的抗拉强度(最高可达到9.92 MPa)和较好的断裂伸长率(最高可达到
11 .75%), 没有耐酸性。而与戊二醛交联后壳聚糖膜的抗拉强度能达到(96 .64 MPa)和断裂伸长率能达到
(10 .92 %), 耐酸性能也得到了大大提高。

关键词: 壳聚糖 , 交联 , 膜 , 性能

Cite this article

JIANG Zhen-ju,SUN Zhong,WANG Zhou-yu. Research on the Preparation and Performance of Chitosan Membrane[J]. Journal of Petrochemical Universities, 2010, 23(2): 61-63.

蒋珍菊,孙仲,王周玉. 壳聚糖缓释膜的制备及性能研究[J]. 石油化工高等学校学报, 2010, 23(2): 61-63.

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