ＭＰＴ－ＡＥＳ法测定野松茶中的微量元素

辽宁石油化工大学学报 ›› 2012, Vol. 32 ›› Issue (2): 8-11.

ＭＰＴ－ＡＥＳ法测定野松茶中的微量元素

赵文涛^１，张金生^１＊，李丽华^２，蔚永清^１，林　静^１#br#

１．辽宁石油化工大学化学与材料科学学院，辽宁抚顺１１３００１；
２．辽宁石油化工大学石油化工学院，辽宁抚顺１１３００１

收稿日期:2012-01-04 出版日期:2012-06-25 发布日期:2017-07-06
作者简介:赵文涛（１９８４－），男，内蒙古通辽市，在读硕士

Determination the Trace Elements in Wild Pine Tea by MPT-AES

ZHAO Wen-tao¹, ZHANG Jin-sheng^1*, LI Li-hua², YU Yong-qing¹, LIN Jing¹

1.School of Chemistry and Material Science, Liaoning Shihua University, Fushun Liaoning 113001, P.R.China;  2.School of Petrochemical Engineering, Liaoning Shihua University, Fushun Liaoning 113001, P.R.China

Received:2012-01-04 Published:2012-06-25 Online:2017-07-06

摘要/Abstract

摘要： 采用微波等离子体炬原子发射光谱法（ＭＰＴ－ＡＥＳ）测定野松茶中的Ｃｕ、Ｚｎ、Ｍｎ、Ｆｅ、Ｍｇ、Ｃａ６种微量元素，在优化各项实验参数基础上，考察了酸干扰和共存离子的干扰。该方法下Ｃｕ、Ｚｎ、Ｍｎ、Ｆｅ、Ｍｇ、Ｃａ的检出限分别为３．６、７．７、６．１、１４．１、４．７、５．６ｎｇ／ｍＬ，方法精密度（ＲＳＤ）为１．０５％～６．４６％，回收率为９７．２５％～１０３．３７％。结果表明此方法简便、准确、分析速度快，是一种切实可行的分析方法。

关键词: 微波等离子体炬原子发射光谱法 , 　野松茶 , 　微量元素

Abstract: The method for the determination of copper, zinc, manganese, iron, magnesium, calcium in wild pine tea by microwave plasma torch-atomic emission spectrometry (MPT-AES) was developed. The effect of nitric acid concentration in the sample solution and co-ionized elements on the emission intensity of copper, zinc, manganese, iron, magnesium and calcium was investigated in detail. The experimental conditions were optimized and showed that the detection limits of metal Cu, Zn, Mn, Fe, Mg and Ca are 3.6, 7.7, 6.1, 14.1, 0.5 and 0.9 ng/mL, respectively, and the RSD of the method is between 1.05%～6.46%, the recoveries are 97.25%～103.37%. This demonstrated that the proposed method is simple, accuracy and efficient, providing a well-established analytical method．

Key words: Microwave plasma torch-atomic emission spectrometry(MPT-AES) , Wild pine tea , Trace element

赵文涛，张金生，李丽华，蔚永清，林　静. ＭＰＴ－ＡＥＳ法测定野松茶中的微量元素[J]. 辽宁石油化工大学学报, 2012, 32(2): 8-11.

ZHAO Wen-tao, ZHANG Jin-sheng, LI Li-hua, YU Yong-qing, LIN Jing. Determination the Trace Elements in Wild Pine Tea by MPT-AES[J]. Journal of Liaoning Petrochemical University, 2012, 32(2): 8-11.