Journal of Petrochemical Universities
Annual Contents
Journal of Petrochemical Universities 2016 Vol.29
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  The Relationship between Viscosity and Sound Velocity of Straight Chain Alkanes
Sun Qiang, Wang Dan, Guo Xuqiang, Liu Aixian, Liu Xiaodong
Abstract316)      PDF (2754KB)(70)      
 

The calculation models for crude oil viscosityare complex because of the determination of physical data,the limited calculation accuracy and application scope. Consequently, some representative straight chain alkanes were taken as model compounds of crude oil, and their viscosity and sound velocity were measured under different temperatures and pressures in this work. The influences of temperature and pressure on the sound velocity of straight chain alkanes were investigated, and the correlation model between viscosity and sound velocity was built on the base of experimental results. The experimental results indicated that the sound velocity of straight chain alkaneslinearly decreased with the increase of temperature and the decrease of pressure. The relationship between viscosity and sound velocity of alkanes was exponential type, and the viscosity sound velocity correlation model was applied to three different oils in Jidong Oilfield. The calculation results demonstrated a satisfactory applicability of the model. So, a feasible method was provided to reduce the dependence of conventional viscosity models on the physical property parameters.

2016, 29 (1): 1-5. DOI: 10.3969/j.issn.1006-396X.2016.01.001
The Effect of Temperature on Moisture Inverted Point and Viscous Ultiples
He Wenyuan, Hao Qingyan, Li Meirong, Meng Qiuyu,Yu Guangsong
Abstract536)      PDF (2615KB)(529)      
Two ordinary heavy oils and three super heavy oils in shengli oil field are used to study and the effect of temperature and viscosity on the moisture inverted point and the viscous multiples. The results show that the inverted point increases with increasing of the temperature, and the viscous multiples of the inverted point also increases. While the viscous multiples of the same moisture content firstincreases and then decreases. Comparing the inverted point and viscous multiples, it is found that the on e which has low viscosity will have high inverted point, low viscous multiples of the same moisture content and high viscous multiples of the inverted point.
2016, 29 (1): 6-9. DOI: 10.3969/j.issn.1006-396X.2016.01.002
Adsorption and Diffusion Behavior of Benzene in NaY Zeolite by Frequency Response Technique
hao Hua, Song Lijuan, Sun Zhaolin, Qin Yucai
Abstract478)      PDF (3035KB)(303)      
Adsorption and diffusion behavior of benzene in NaY zeolite are studied by using the frequency response method. The TG/DTG curves and Py FTIR technique are used to analyze the adsorption and diffusion mechanism of benzene on NaY. The results indicate that NaY zeolite contains two kinds of acidic centers, namely, the weak B acid and weak L acid sites. And L acid sites are in a dominant position. There are two adsorption interactions on NaY zeolite at 333 K and 423 K, the adsorption of low frequency through the π electronic interactions and high frequency of adsorption belong to pore filling. Adsorption is still the controlling stepat 573 K. However, diffusion is the controlling step on NaY at 623 K, indicating that weak adsorption results in easier desorption and easier diffusion of aromatic molecules on NaY, there by improving the performance of the hydro cracking reaction.
2016, 29 (1): 10-13. DOI: 10.3969/j.issn.1006-396X.2016.01.003
Enhancing Super Extra Heavy Oil Recovery by Using High Temperature Resistant Enhanced Foam System
Wang Chunzhi,Li Zhaomin,Li Songyan,Li Binfei,Zhang Chao,Wang Fei
Abstract530)      PDF (4608KB)(429)      
After multiple rounds of steam huff and puff processes, problems of excessive steam injection pressure, a large heat loss, a small sweep range of steam, and steam channeling arise, thus severely affecting the effective utilization of the oil reservoir. To solve these problems, one dimensional and three dimensional (3D) physical simulation tools were used to study the plugging performance of high temperature composite foamsby adding tanning extract and alkali lignin. The influence of reservoir temperature, salinity of formation water, and injection methods was investigated. The experimental results show that the foam can produce a synergistic effect with both the gel systems, indicating that the gel increases the stability of the foam. The foam can transfer more gel into the high permeability formation, thus efficiently controlling the foam. The 3D physical simulation experiments indicate that both the systems enhance the recovery of heavy oil reservoir and reduce its moisture content significantly using steam injection. The method involving tannin extract foam and steam injection increased the recovery by 20% compared to the foam involving only steam injection. The method involving alkali lignin foam and steam injection increased the recovery by 11%.
2016, 29 (1): 14-20. DOI: 10.3969/j.issn.1006-396X.2016.01.004
 

Key Techniques of Horizontal Well Design Platform in Tight Sandstone and Their Applications: A Case Study into Fuyu Oil Layer of Northern Songliao Basin

Wang Xianhua
Abstract266)      PDF (18349KB)(9)      
 

Considering the geological features of the tight sandstone reservoir of Fuyu oil layer, Northern Songliao Basin, some key techniques of horizontal well design platform were developed based on the geological studies in the pilot development projects. These techniques attached importance to the key controls in geological design of horizontal wells by using such techniques as accurate delineation of the structural features in depth domain, fine characterization of sweet spot sandstone distribution, quantitatively fine description of channel sandstone geometry and optimum horizontal well design based on refine 3D geological model, which laid the solid foundation for locating the horizontal wells. The successful results were attained in horizontal well drilling in the primary stage of pilot project. The availability of the reservoir of tight channel sandstone within Fuyu oil layer was raised, the production of individual well and single well controlled reserves were greatly enhanced combining with volumetric fracturing stimulation, and support for economically tapping the tight oil in Daqing oilfield was securing.

2016, 29 (1): 21-30. DOI: 10.3969/j.issn.1006-396X.2016.01.005
 

Nitrogen Foam Profile Control and Displacement Technology Applied in Naturally Fractured Low Permeability Reservoir

Zhou Zhibin, Wang Jiexiang, Wang Tengfei
Abstract310)      PDF (1772KB)(39)      
 

Water channeling is a serious problem during the water flooding of naturally fractured low permeability reservoir. To solve the problem, nitrogen foam profile control and displacement technology were researched applying both experimental and simulation methods. The sealing capacity and oil displacement capacity of nitrogen foam were the main research objects. The results showed that nitrogen foam could reduce water cut and increase oil recovery significantly. After plugging the interconnected fracture, the swept volume of flooding liquid and oil recovery would be increased obviously. In the experimental research, oil recovery efficiency was increased by more than 10% after injection of nitrogen foam. The injection of nitrogen foam was flexile and convenient when applied in field construction, and the nitrogen foam profile control and displacement technology were suitable for EOR of naturally fractured low permeability reservoirs.

2016, 29 (1): 31-34. DOI: 10.3969/j.issn.1006-396X.2016.01.006
Profile Control and Flooding Effect of Alternate Injection of Cr3+ Polymer Gel and Water and Its Mechanism Analysis: Taking the Bohai Oilfield as an Example
Zhang Baoyan, Lu Xiangguo, Xie Kun, Liu Yigang, Zhang Yunbao
Abstract305)      PDF (2648KB)(64)      
Aiming at technical demand on relieving the reverse of imbibition profile, displacement effect of alternate injection of Cr3+ polymer gel and water was studied, taking reservoir of Bohai oilfield as simulation object, regarding injection pressure, water content and recovery efficiency as evaluation index. Results showed that as the displacement agent flowed into the medium and low permeability layer, on the one hand, the swept volume was magnified. On the other hand, seepage resistance and start up pressure of imbibition were increased, thus resulting in the reverse of the imbibition profile. Once the alternate injection of Cr3+ polymer gel and water was adopted, polymer solution could get priority to flow into the high permeable layer and block off it, then subsequent water flowed into medium and low permeability layers to displace the oil. Therefore the phenomenon of the reverse of imbibition profile was relieved or even eliminated. Once the alternate injection of C3+ polymer gel and water was conducted in A22 injection well in LD5 - 2 Oilfield, injection pressure get increased, which was good for enlarging sweep volume effect.
2016, 29 (1): 35-40. DOI: 10.3969/j.issn.1006-396X.2016.01.007
 

Improvement of Inhomogeneous Producing Degree for Polymer Flooding Layers Applying Step Perforation

Yin Daiyin, Zhou Xuan
Abstract261)      PDF (2877KB)(38)      
 

A method which applies step perforation to improve the effect of polymer flooding is presented against the problems of poor producing degree of low permeability, remaining oil in the inner thick oil layer abounds, and uneven vertical producing degree. After water flooding, the thick layers are perforated selectively followed by water flooding potential tapping, and the polymer flooding is performed ultimately. By carrying out laboratory physical oil displacement experiment of three tube parallel cores and applying theoretical formulas, reasonable polymer injection parameters are determined and the impacts of polymer flooding after step perforation on development effectiveness are also studied. The results showed that the better effect of polymer flooding was obtained by using big pre slug, high molecular weight polymer, and echelon descending concentration slug combinations. And projects which had adopted step perforation showed a bigger producing degree on low permeability layers and a better effectiveness on polymer flooding compared to the ones not adopted step perforation. The ultimate recovery was increased by 1.28%.

2016, 29 (1): 41-45. DOI: 10.3969/j.issn.1006-396X.2016.01.008
Performance of " β - CD/Hydrophobic Associating Water Solute Polymer" and Its Seepage Flow Characteristics: Take the Third Southern Part Reservoir of Daqing Oilfiled as Research Object
Cao Weijia, Lu Xiangguo, Yuan Shengwang, Jiang Xiaolei
Abstract267)      PDF (2454KB)(65)      
Hydrophobic associating water solute polymer has excellent viscosity and salt resistance, but the adaptability between its "mesh" molecular aggregation and reservoir pore throat causes attention of petroleum technology staffs. Aimed at the actual need, gui ding by reservoir engineering, physical chemistry and organic chemistry, the adaptability with hydrophobic associating polymer and experimental effect on southern reservoir were carried out using instrumental analysis, chemical analysis and physical simula tion as technical means. Results showed that with the increasing of β - CD, the viscosity of hydrophobic associating water solute polymer solution first reduced quickly and then got stable. When the concentration of β - CD was 0.07%, hydrophobic association between groups was completely suppressed, and the viscosity of polymer solution was bulk viscosity. In addition, the aggregation size of hydrophobic associating polymer molecular was decreased by β - CD, and the entering extent to reservoir of the polymer molecular group was expanded, thus the adaptability of hydrophobic associating water solute polymer with reservoir was improved.
2016, 29 (1): 46-52. DOI: 10.3969/j.issn.1006-396X.2016.01.009
The Fractal Feature of the Pore Structure for High Coal Rank Coal Porous Media
Jia Huimin
Abstract431)      PDF (2301KB)(448)      
An effective way to describe the heterogeneity of pore structure quantitatively is provided by fractal theory,and the special pore cleat dual pore structure of coal rock makes iturgent to research further whether coal rock bears fractal feature and how to describe it. Using the present fractal feature research way and the fractal dimensions calculation way of sandstone as reference, mercury injection curvesof five pieces of coal porous media are carefully studied.The results show that the coal porous media bears fractal features in three separate zones, r<0.1 μ m 0.1 μ m<r<10 μ m and r>10 μ m. And for each zone,these pores are micro pores and small pores, middle pores and big pores and cleat (r>10 μ m)correspondingly. In general trend, the greater the fra ctal dimension is, the smaller the values of porosity and permeability and the worse the sorting and heterogeneity features of pores are. For different radius zones of a certain sample,the greater the fractal dimension is, the greater the heterogeneity of its pore radiusis.
2016, 29 (1): 53-56. DOI: 10.3969/j.issn.1006-396X.2016.01.010
 

Mechanism and Oil Displacement of Heavy Oil Emulsification and Viscosity ReducerA Case Study on Heavy Oil Reservoir and Fluid Conditions of Bohai Oilfield

Xu Guorui, Li Xiang, Xie Kun
Abstract276)      PDF (2593KB)(58)      
 

In order to further explore the mechanism of increasing oil and decreasing viscosity of heavy oil emulsification and viscosity reducer, experimental studies on oil displacement of heavy oil emulsification and viscosity reducer and its influencing factors have been carried out. Viscosity reducer was screened and related performance was evaluated.The viscosity and recovery efficiency were used as evaluation indexaccording to the geological characteristics and fluid properties in Bohai reservoir. The results showed that, the mechanism of decreasing viscosity of three kinds of viscosity reducer was forming oil in water emulsion, and the viscosity reduction effect of viscosity reducer 2 was best among three kinds of viscosity reducer. Oil water emulsion gradually changed from oil in water (O/W) into water in oil(W/O) type and the viscosity was increased when the water content in emulsion decreased, eventually exceeding that of crude oil. Besides, with the heavy oil reservoir hetergeneity increasing, oil displacement of viscosity reducer got better. Oil displacement of viscosity reducer got worse with the increasing of curde oil viscosity, so the recovery amplification can be increased through preprocessing on viscosity reduction before similarty viscosity reducer was used.

2016, 29 (1): 57-62. DOI: 10.3969/j.issn.1006-396X.2016.01.011
 

Compound Flocculant System for Oil Bearing Sewage Containing Polymer in GD Oilfield

Zhang Yingping
Abstract298)      PDF (2187KB)(64)      
 

Oil bearing sewage containing polymer in GD Oilfield has the properties of high viscosity, high oil content and more suspended particles, and the conventional single flocculating agent has the disadvantages of high dosage, loose coagulation and high cost. Oil removal rate and removal of turbidity were chosen as the evaluation values in this test, and flask experiment was used to evaluate the sewage processing effect of three inorganic flocculants and two organic polymer flocculants. Inorganic flocculant of poly (aluminium ferric chloride) with the concentration of 100 mg/L and organic polymer flocculant of PAM 4 with the concentration of 40 mg/L were respectively selected as the best flocculant. The oil removal rate and removal of turbidity of waste water were 92.3% and 90.7% respectively when poly (aluminium ferric chloride) and PAM 4 were used to dispose oilfield waste water. Some influencing factors such as temperature, pH value and settling time were investigated. The experimental results showed that the oil removal rate and removal of turbidity of oilfield waste water which was disposed by using compound flocculant system were the best when temperature of waste water was 40~60 , pH value of waste water was 6~9 and the settling time was longerThe compound flocculant system has strong prospect in the processing of oil bearing sewage containing polymer.

2016, 29 (1): 63-66. DOI: 10.3969/j.issn.1006-396X.2016.01.012
 

Adsorption and Drag Reduction Performance Research of Molecular Film on the Rock Surface

Li Rongqiang, Wang Jianzhong, Qi Chunjie, Chen Shudong
Abstract258)      PDF (3161KB)(96)      
 

The wettability and microstructure characteristics can be changed by molecular film technology through injecting molecular film reagent into the reservoir micro pores, and the purpose of reducing injection pressure and improving water injection total is achieved. The adsorption capacity comparison between molecular films to rock surface with water molecular to rock surface was studied, and it was revealed that the molecular film took advantage in competition, then adsorbed in rock surface and formed molecule layer. Based on it, the application conditions and its change rules were explored then the molecular drag reduction mechanism from reducing the boundary layer effect and friction was revealed. At the last the property of the molecules film drag reduction was studied.

2016, 29 (1): 67-71. DOI: 10.3969/j.issn.1006-396X.2016.01.013
 

Finite Element Analysis of Sealing Performance of Non Standard Octagonal Gasket on Hydrotreating Reactor

Chen Song, Liu Jinchun, Yang Yufeng, Jing Pengfei, Xie Yujun
Abstract259)      PDF (3036KB)(35)      
 

Aiming at non standard octagonal gasket used in hydrotreating reactor. Ansys was used to calculate the contact stress on the sealing surface during the hydrostatic pressure test, and the causes of the different contact stress on each sealing surface were analyzed. The results showed that the contact stress down to the trough when the test pressure was the highest, the maximum stress on the inner side of gasket was away from the center of gasket, and the outer situation was in contrast to it. Variation of gasket sealing surface contact stress provides a reference to the analysis and evaluation of other non standard seal structure.

2016, 29 (1): 72-75. DOI: 10.3969/j.issn.1006-396X.2016.01.014
 
Fault Diagnosis of Electric Submersible Pump Based on BP Neural Network
Peng Kexiang
Abstract325)      PDF (1250KB)(388)      
 

Current card is the main basis of electric submersible pump well fault diagnosis. At present, the diagnosis of electric pumping wells is mainly completed by technical workers. It is difficult to achieve rapid mass diagnosis, and the diagnosis results are greatly influenced by engineer technology level. Therefore the application of BP neural network for fault diagnosis of electric submersible pump is put forward. First of all, different pump current cards are collected, and sample library is established. The eigenvalues of the different pump current card are gathered and trained according to certain principles. After completion of training a weight matrix is got, and the current card characteristic values and weights matrix of similarity is calculated. Through computer programming application, the method can be proved to make electric pump diagnosis accurately and rapidly.

2016, 29 (1): 76-79. DOI: 10.3969/j.issn.1006-396X.2016.01.015
Wax Deposition of Tangyan Crude Oil Pipeline
Zhao Dan, Huang Qiyu, Lyu Zhijuan, Lyu Mingkuan
Abstract546)      PDF (2830KB)(416)      
A number of crude oils is transported by Tangyan crude oil pipeline with frequent switch and thus wax deposition prediction is difficult. In this paper, wax deposition rates of different transported crudes along Tangyan pipeline in different seasons are predicted by using the unified wax deposition model based on crude properties. The thickness and distribution of wax deposition are forecasted, which provide a theoretical basis for the pigging operation securely. The results show that the wax deposition rates of different crudes in different seasons are various. Wax deposition along Tangyan pipeline mostly happens in winter and seldom happens in summer. Wax deposition of Aisipo and Maxila crude oil is less than that of Jienuo and Shazhong crude oil. The distribution of wax deposition along the pipelineis uneven. Wax deposition mainly accumulates in the inlets of the pump stations. When there is little variation of pipeline operation stress, the pressure drop in the unit length increases rapidly in the position where wax deposition is serious. Pressure effect may cause potential security risks in the pipeline. It is suggested that the pigging operation should be conducted in each autumn.
2016, 29 (1): 80-85. DOI: 10.3969/j.issn.1006-396X.2016.01.016
 

Numerical Simulation of Sand Depositional Rule in Subsea Multiphase Pipeline

Zhang Wenxin, Zhou Xiaohong, Chen Hongju
Abstract271)      PDF (7306KB)(29)      
 

Sand deposit will be formedinside of subsea multiphase pipeline after operating for a period of time, which will lead to diminution of passable area, reduction of inhibitor efficiency, acceleration of corrosion, and even cause the PIG block accidents. In this article, the geometrical model and physical model with field dataare set up building upon the subsea multiphase pipeline from platform A to B in a group of offshore oil and gas fields.Numerical simulations by FLUENT are performed in order to study the sand depositional rule of straight section and bend section according to the variation of parameters such as sand content, particle size, density and flow rate. The research shows that sand depositional amount is positive correlative with and content, particle size, density and negative with flow rate, and the rule of sand depositional maximum position is opposite. The sensitivity of parameters to average sand depositional amount is sand content, flow rate, particle size and density from high to low.

2016, 29 (1): 86-92. DOI: 10.3969/j.issn.1006-396X.2016.01.017
 

The Research Progress of Gas Desorption Technology

Feng Chunbo, Yuan Ye, Xing Xiaokai
Abstract265)      PDF (1282KB)(88)      
 

Rapid and efficient desorption of CO2 from produced liquid has become a key issue which is addressed urgently in the gathering and transporting system of CO2 drive oilfield in China. Main theories of gas desorption are introduced and the features of traditional desorption technology, membrane desorption technology and ultrasonic desorption technology are analyzed in this paper.On the basis of which, defects of all kinds of desorption technologies are pointed out, and the direction of the gas desorption research is proposed. In addition, research progress of ultrasonic desorption, based on the self built experimental device of ultrasound promoting the gas desorption from the CO2 drive produced liquid, is introduced. Then, the combination of the new desorption technology and the traditional desorption is suggested to be applied to the CO2 desorption of produced liquid.

2016, 29 (1): 93-98. DOI: 10.3969/j.issn.1006-396X.2016.01.018
The Application of Sn - Bi - Co AC Catalysts for Acetylene Hydrochlorination
Gao Shiliang, Sun Xi, Lyu Zhongling, Qin Yucai, Zhang Xiaotong, Song Lijuan
Abstract285)      PDF (2738KB)(87)      
Using active carbon as carrier, SnCl4 based non mercury catalysts, including Sn@AC, Sn - Bi@AC, Sn - Bi - Co@AC, were synthesized by adding different content of BiCl3 and CoCl3. The catalysts were evaluated in acetylene hydrochlorination atmospheric fixed bed reactor. The results showed that the catalytic properties of synthetic three component catalysts were optimal on the proportion of 10%SnCl4, 5%BiCl3 and 10%CoCl3. Acetylene's conversion rate was more than 90% and the selectivity of vinyl chloride was a round 95% within the reaction time of 100 h. Through the XRD and physical adsorption instrument, catalyst microstructures were characterized. Coconut shell activated carbon's specific surface area and pore size was significant increased after nitric acid t reatment; adding component BiCl3 and CoCl3 could make the coke phenomenon on catalytic surface weakened.
2016, 29 (2): 1-5. DOI: 10.3969/j.issn.1006-396X.2016.02.001
Synthesis and Properties of the Unsaturated Polyester Polyurethane with Lateral Base Double Bonds
Wang Chuanxing, Liu Junkai, Xu Qinhong, Gao Chuanhui, Wu Yumin, Hou Baorong
Abstract551)      PDF (2375KB)(807)      
With itaconic acid (IA) and 1,4 butanediol (BDO) as the raw materials, the resultant hydroxyl terminated aliphatic unsaturated polyesters (PBI) were prepared. The unsaturated polyurethane was prepared with PBI as the soft segment and toluene diisocynate (T DI) as the hard segment. The effect of its reaction conditions on the mechanical properties of the unsaturated polyurethane was also investigated. It was found that the film products with the optimum properties were obtained under the material mass ratio o f TDI and PBI 1 1.5, the reaction temperature 80 , optimum reaction time 2 h, with dibutyltin dilaurate in an amount of 1% as the catalyst. Combining with benzoyl peroxide in an amount of 1%,as an initiator, the film of the unsaturated polyurethane was smooth, transparent and level. The hardness was 6H, and the adhesion property was A grade.
2016, 29 (2): 6-12. DOI: 10.3969/j.issn.1006-396X.2016.02.002
Preperation and Hydrodearomatization Performance of NiWP Catalyst Containing Hierarchical H β
Wang Yujia, Yue Yuan, Lu Cong, Wei Min
Abstract344)      PDF (2437KB)(84)      
 

The hierarchically mesoporous Hβ zeolite was synthesized by alkali treatment to commercial Hβ zeolite in NaOH solution. The composite carrier was prepared by mixing the hierarchical Hβ zeolite and Al2O3.The hierarchical NiWP/HβAl2O3 catalysts were prepared by incipient wetness impregnation method, and characterized by means of XRD, BET and TEM. The hydrodearomatization of the prepared NiWP/HβAl2O3 catalyst was evaluated in a miniature fixed bed reactor with fluid catalytic cracking diesel as raw material. The results suggested that the prepared NiWP/HβAl2O3 catalyst has an excellent hydrodearomatization activity, and under the condition of the reaction temperature 360 , reaction pressure 8.0 MPa, hydrogen to oil volumetric ratio 800 and liquid hourly space velocity 1.0 h-1, the cetane number was increased from 7.21 of feed to 46.96 of product.

2016, 29 (2): 13-17. DOI: 10.3969/j.issn.1006-396X.2016.02.003
 

Effects of Binder Component to Adsorptive Desulfurization Catalyst for FCC Gasoline on Desulfurization Performance and Mechanical Strength

Chen Yifei Ji Dekun, Ding Fuchen,Chi Yaoling, Yi Yufeng
Abstract339)      PDF (2551KB)(58)      
 

Using Al2O3, HNO3 and other components as binder component, Ni as active component, ZnO as sulfur storage material, the adsorptive desulfurization catalyst was prepared by equal volume impregnation method. The effects of the Al/Si mass ratio, kneading time of the supporter, adding quality percentage of nitric acid and binder component on catalysts desulfurization performance and mechanical strength were investigated. The results showed that the catalysts desulfurization performancewas improved when the adding quality of nitric acid, pseudo boehmite and kieselguhr was increased. The desulfurization performance was increased and then decreased with increasing of Al/Si mass ratio, increased and then kept stable with increasing of kneading time. The catalysts mechanical strength was improved when the Al/Si mass ratio increased, the adding quantity of nitric acid decreased, pseudo boehmite and kieselguhr increased and the kneading time increased.

2016, 29 (2): 18-22. DOI: 10.3969/j.issn.1006-396X.2016.02.004
 

The Effect of Bromide Process on the Gel Content of Brominated Butyl Rubber

Dong Mimi, Guo Wenli, Li Shuxin, Chang Jinjie, Zhang Tao
Abstract306)      PDF (1515KB)(62)      
 

Gel content has a certain impact on the immanent quality of rubber products and processing performance. Therefore, it is crucial for brominated butyl rubber to control the gel content. Brominated butyl rubber (BIIR) was prepared by solution method and the effect of the brominated process such as bromination temperature, additives, bromination time and bromide agent on the gel content of BIIR was investigated. The results show that the appropriate reaction temperature is conducive to the control of the gel content. Gel content will increase with the increasing of the concentration of time and bromide agent. The additives can lower the gel content.

2016, 29 (2): 23-26. DOI: 10.3969/j.issn.1006-396X.2016.02.005
 

Experimental Study on the Cyclic Pressure Loss of Pump Injected Reverse Circulation Drilling

Che Yang, Zhou Jinhui, Wu Han, Cheng Jiaqi
Abstract284)           
 

Pump injected reverse circulation drilling is a new drilling method. It has lots of advantages (such as cleaned hole and high ROP) compared with previous method, which can be used in drilling complex structural well. As we all know, cyclic pressure loss is one of the most important topics in drilling. The laws of cyclic pressure loss in different nozzles or mud parameters are studied experimentally in lab. The paper analyses the major factors affected cyclic pressure loss, according to results of the simulated experiment. It comes to the conclusions that the area of the bit nozzles should be a half of the drilling stem. And the edge of the bit is the best position to place the bit nozzles. At the same time, the cyclic pressure loss can be higher while the density of drilling fluid increases. However, the density doesnt seem to affect the best arrangement of bit nozzles. Theoretical basis is provided for optimized design of pump injected reverse drilling bit nozzles.

2016, 29 (2): 27-31. DOI: 10.3969/j.issn.1006-396X.2016.02.006
 

Blockage Reason of Polymer Injection Wells in Xingnan Oilfield and Determination of the Plug Removal Agent Formula

Cao Guangsheng, Li Chuncheng, Wang Tingting, Wang Guilong, Zhang Xianqiang
Abstract399)      PDF (2791KB)(80)      
 

According to the problems of that the serious blockage of polymer injection wells, the high injection pressure and the bad effect of polymer injection in Xingnan oilfield, the polymer and water of a block in Xingnan oilfield was adopted to carry out the laboratory experiments on simulation of polymer flooding and plugging and then the reason of blockage was found out.  The results show that the polymer and mechanical impurities are the main factors to cause the pore blockage, and the lower the permeability, the more serious the blockage. Aiming at the blockage reason, laboratory experiment study on the formula of plug removal agent was carried out. Finally the multiple plug removal agent consists of agent A, B and C was determined. On the basis of optimizing the mass fraction of each agent, the injection volume and the injection order, the broken down rate of formations can reach 102.41%~124.77% with this plugging removal agent formula.

2016, 29 (2): 32-36. DOI: 10.3969/j.issn.1006-396X.2016.02.007
 

Determination of Original Oil Saturation for Chang 8 Layer in Northeastern Zhiluo Oilfield

Wang Zhongyuan, Wang Guicheng, Chang Weili, Wei Xiaodi
Abstract308)      PDF (2874KB)(53)      
 

Chang 8 layer in northeastern Zhiluo oilfield of Ordos basin is a structural lithologic reservoir controlled chiefly by lithology with many oil water layers. There are many oil water layers in this region. Aiming at this characteristic, on the basis of the methods of pressure coring, mercury injection and log data interpretation, the data of relative permeability analysis is used to to interpret and revise the original oil saturation in the area. The four methods are used to calculate the original oil saturation in Chang 8 layer of northeastern Zhiluo oilfield and the advantages and disadvantages of each method are analysized. The reasonable original oil saturation in Chang 8 layer of this area is determined, and the accuracy of calculation of reserves is improved. The method of relative permeability analysis data is the best method to calculate the original oil saturation in this area, eventually the original oil saturation value is 45.6%.

2016, 29 (2): 37-43. DOI: 10.3969/j.issn.1006-396X.2016.02.008
 

The Initial Cracking Point of Multi Branch Hydraulic Fracture Temporary Plugging

Xia Chong, Liao Xuan, Liu Jingcheng
Abstract374)      PDF (3468KB)(48)      
 

The seam crack point of multiple branch seam fracturing is not clear. Based on the theory of porous media of fluid solid coupling mode, Comsol software was used to simulate branch seam fracturing process using finite element simulation. The changing law of stress concentration of seam crack point and shaft crack point was analysized under the condition of different stress difference it was found that with the increase of net pressure on the seam, there was a difference which distinguished between crack priorities. By controlling the net pressure change within joint, the crack priorities was adjusted, the number of multi branch fracture was controlled, and the multi branch seam hydraulic pressure of the complexity of the fracture network was ensured. Calculation analysis of hailaer oil field on the spot was used to adjust the net pressure inside seam. The result of construction was same with simulation, and can be used to guide the construction to improve the success rate of multi branch seam hydraulic fracturing.

2016, 29 (2): 44-48. DOI: 10.3969/j.issn.1006-396X.2016.02.009
 

Study and Application of Multi Slug Compounding Profile Control and Flooding Technology in Zhidan Shuanghe Oil Block

Wang Weibo, Yang Yongchao, Kang Xiaoyu
Abstract289)      PDF (1520KB)(51)      
 

Aimming at the problem of shorter validity period during early flooding stage for low permeability fractured reservoirs in Shuanghe oil block from Zhidan oil field, a technical study and application of multistage compounding flooding was carried out. Based on the profile and flooding mechanism of different slugs, the agents were screened and evaluated indoor. Consumption volume, slug combinations, displacement volume and pressure in flooding scheme were optimized. Field test for SH 69 well proved that using the multi slug compound flooding way of polymer protected slug + high cure system + delayed swelling gel system + delayed crosslinking gel system, the climbing pressure was 2.2 MPa, the start up pressure of injection well was increased with 0.72 MPa effectively, and injectivity index was reduced with 1.9 m3/(d·MPa), which had an obvious effect of controlling water and increasing oil for corresponding wells. The valid period for this type of flooding was up to six months or more, which achieved the integration process of control and flooding, realizing the target of adjusting water injection profile and increasing oil recovery.

2016, 29 (2): 49-54. DOI: 10.3969/j.issn.1006-396X.2016.02.010
The Deviation Revise in High Temperature Gas Well Production Testing Water Contents Result
Lin Fei,Deng Keshu,Ma Jie,Deng Chuanzhong
Abstract380)      PDF (1159KB)(305)      
 

Generally, water production of natural gas well is important in the gas field development, and parts of production water of high temperature gas wells exist in saturated water vapor form, leading to measurement result deviation. In order to reduce the  water measurement result deviation of high temperature gas well production, it is necessary to calculate the saturation water content of natural gas and correct the deviation from production water measurement. Through the analysis of natural gas water content calculation method principle, and the contrast in the practical application effect of Y13 gas field, the method of semi empirical formula with theoretical derivation is suitable for the actual Y13 gas field. According to this method, the average deviation can be decreased from 60% to less than 6%.

2016, 29 (2): 55-59. DOI: 10.3969/j.issn.1006-396X.2016.02.011
 

Research on Oil Displacement Feasibility of Polymer Solution Diluted by Polymer Flooding Sewage

Zhang Jihong, Xu Sining
Abstract306)      PDF (2035KB)(46)      
 

In the process of polymer flooding in daqing oilfield, there are some problems such as water consumption growing tensions, sewage treatment increasing more differences and the problem of injecting sewage becoming serious. Using the produced sewage instead of water to dilute polymer solution flooding will be widely attached. Aiming at the characteristics of polymer flooding sewage depth by polymer flooding sewage and sewage water quality analysis, polymer flooding sewage by oxygen exposure and sterilization was used to study flow characteristics and oil displacement effect. Results show that, compared with deep treatment sewage, residual resistance coefficient with polymer solution is high after polymer flooding sewage dilution, the ability to reduce water phase permeability is enhanced, and recovery factor is improved. Under the same conditions of permeability, molecular weight, concentration, and depth of sewage displacement effect of polymer solution is not ideal compared to dilute oil, and the value of recovery efficiency  differs by about 1%. The same effect with the polymer flooding deeply produced by sewage dilutes can be achieved if the concentration of polymer solution diluted by the polymer flooding sewage is increased.

2016, 29 (2): 60-64. DOI: 10.3969/j.issn.1006-396X.2016.02.012
Experimental Method about Enhancing Oil Recovery after Alkaline/Surfactant/Polymer Flooding:Take Xingshugang Oilfield in Daqing as Research Object
Wang Zijian, Lu Xiangguo, Jiang Xiaolei, Zhang Yuexian, Song Ru’e
Abstract400)      PDF (2932KB)(315)      
In order to explore a method of further enhancing oil recovery after alkaline/surfactant/polymer flooding, taking Xingshugang oilfield in Daqing as an experiment platform and regarding oil recovery, water content and injection pressure as evaluation indicators on enhancing oil recovery, an experiment was conducted under the condition of the constant temperature and constant pressure. The results showed that alkali/surfactant/polymer with strong base system, surfactant polymer system and alkali/surfactant/polymer with weak base system could all further enhance oil recovery, and the effect of high concentration polymer liquor was the best. The greater the subsequent of the injection pressure rose, the more the recovery growth was. Taking into account the constraints of Daqing oilfield reservoir and equipment capacity. Based on the comprehensive consideration of technical and economic effects, aurfactant polymer system has more application prospects.
2016, 29 (2): 65-70. DOI: 10.3969/j.issn.1006-396X.2016.02.013
 

The Effect of Ca2+ and Mg2+ on Polymer/Surfactant Binary Combination: Taking the Reservoirs of Kongnan Block in Dagang Oilfield as an Example

Su Xin, Lu Xiangguo, Cao Weijia, Yang Huaijun, Zhang Jie
Abstract295)      PDF (1787KB)(43)      
In recent years, more attention was paid to unconventional reservoir development due to the increase in oil consumption and the reduction of new proved reserves. The reservoirs of Kongnan Block in Dagang Oilfield belong to the high temperature, high salinity and hypercoagulable reservoirs. In order to improve the effect of polymer/surfactant binary combination flooding, the effect of solvent water treatment on polymer/surfactant binary combination based on Kongnan Block of Dagang Oilfield reservoir geologic al characteristics and fluid properties was studied. The results show that, elimination of the Ca2+ and Mg2+ in the injected water can enhance the association of hydrophobic associated polymer and improve the viscosity and flow turning ability of polymer/surfactant binary combination. After adding into the polymer/surfactant binary combination, not only can eliminate the adverse effect of Ca2+ and Mg2+ on the salt resistance of hydrophobic associated polymer, but also can form a large number of particles which can further enhance flow turning ability by entering reservoir porosity. Compared with injected water and softened water, the flow turning ability and recovery of the polymer/surfactant binary combination which is configured by softened water with particles are better.
2016, 29 (2): 71-75. DOI: 10.3969/j.issn.1006-396X.2016.02.014
Performance of End Face Seal with Inclined Diamond Pores
Cheng Xiangping, Meng Xiangkai, Peng Xudong, Zhang Youliang, Kang Linping
Abstract451)      PDF (6280KB)(351)      
Based on a liquid lubrication theory, influence of operating parameters and texturing parameters on open force, film stiffness and leakage was numerically investigated. Then upstream and downstream pumping principles of the inclined diamond pores were discussed. Results show that the liquid seal with bidirectional inclined diamond pores had larger hydrodynamic open force, more reliable liquid membrane stability and lower leakage than those with unidirectional. At low speed, bidirectional inclined diamond pores texture can make seal end faces opened quickly, and can effectively reduce the friction and wear between two end faces in the startup phase. At the same time, the leakage of the inclined diamond pores texture seal can also be reduced; Under the operation conditions of research, the liquid membrane stability (Self adaptive capacity of the variable conditions) of the non inclined diamonds texture seal was the best in the three (the bidirectional, unidirectional and non inclined diamond pores texture seals); And optimization range of reverse pores ratio, pores inclination angle, pores area rate and pores depth was obtained.
2016, 29 (2): 76-81. DOI: 10.3969/j.issn.1006-396X.2016.02.015
Numerical Simulation Research of Bubble Enhanced Hydrocyclone
Fang Xiangjiu, Chen Jiaqing, Liu Meili, Ji Yipeng, Kong Xianggong
Abstract565)      PDF (5736KB)(589)      
By means of Eulerian Model combined with Discrete Phase Model, the numerical simulation of three phases flow field in bubble enhanced hydrocyclone was performed to analyse the velocity distribution inside the hydrocyclone and the trajectories of oil droplet. The separation efficiency of hydrocyclone after bubble injection was compared with conventional hydrocyclone in different aspects such as partical size, flow rate and oil content in wastewater. The simulation result showed that tangential velocity and axial velocity inside the hydrocyclone after bubble injection were higher than that of conventional hydrocyclone, leading to a quicker escaping time of oil droplet. Meanwhile, bubble injection could increase the separation efficiency of oil droplet above 30 micron by 10% to 20%. The calculation confirmed that bubble injection at inlet could promote the separation performance of hydrocyclone in terms of numerical simulation.
2016, 29 (2): 82-88. DOI: 10.3969/j.issn.1006-396X.2016.02.016
Research on Parametric Modeling of Centrifugal Pump Impeller and Volute Coupling Based on Pro/E
Yue Jian, Hao Jiao, Sun Tie, Zhang Suxiang
Abstract660)      PDF (3636KB)(906)      
The impeller and volute are important parts of centrifugal pump.Their degree of precision and coupling production directly affect the performance of centrifugal pump water conservancy.In order to improve the flow loss generated atthe impeller and volute coupling, Pro/E is taken as the design platform. the analysis and mapping method of impeller and volute Wooden patterns 2D projection are put forward. Combined with Pro/E in the "offset coordinate datum point command" commands, the twisted blade and volute impeller entity modeling precision are realized through Fluent numerical simulation. The pressure and velocity distribution of impeller and volute coupling shows that pressure and velocity are uniform regularity, and head of delivery calculation shows that the design requirements meet design requirement.The analysis results show that this method is not only drawing accurate, but also is fast and flexible, and it can improve the flow loss of the coupling of the impeller and the volute, which lays the foundation for further numerical analysis.
2016, 29 (2): 89-94. DOI: 10.3969/j.issn.1006-396X.2016.02.017
Calculation of Leakage Probability of Pipe Connecting  Flange Based on Monte Carlo Method
Wang Chenglong, Xie Yujun, Wei Quanquan, Yu Xiaoze
Abstract425)      PDF (2634KB)(420)      
Bolted flange joints were simulated with the finite element software Ansys, getting the gasket stress distribution under the condition of the preload and operation, and calculating the gasket stress under different working condition of internal pressure. Due to constant fluctuations in pipeline pressure and the pipe stress complex, the working pressure, temperature, uncertain factors such as their own constraints on its tightness should be fully considered. The Monte Carlo method is used to have reliability analysis in pipeline working pressure fluctuating. Limit equation is created and according to the distribution of the variable type and limit equation using largescale software Matlab is used to repeat random sampling to calculate the probability of bolt flange leakages under different working pressures. The results show that, the additional load produced by working pressure fluctuation will have a very big effect on the bolt flange leak, that must be got seriously enough attention.
2016, 29 (2): 95-98. DOI: 10.3969/j.issn.1006-396X.2016.02.018
Influence of POE on the Aging Properties of SBS Modified Asphalt
Wang Lizhi, Li Xiaodong, Wang Chengxian, Wang Peng, Zhao Jingyuan, Wei Jianming
Abstract839)      PDF (4929KB)(379)      
For exploring the influence of POE(Poly Olefin Elastomer)on the aging properties of SBS modified asphalt, the index of rheological analysis, fluorescence microscope analysis, as well as the infrared spectroscopy measurement of the SBS modified asphalt, POE/SBS modified asphalt, and its residue after shortterm and longterm aging performance testing were investigate. The results indicated that POE can be compatibilized with the SBS modified asphalt due to its good molecular mobility. In this way, the SBS can be dispersed more homogeneously and be swollen more effectively, through which the aging process is reduced in this compatibility system.
2016, 29 (3): 1-6. DOI: 10.3969/j.issn.1006-396X.2016.03.001
The Morphology Control Research of Paraffin/Melamine Resin Phase Transition Microcapsules
Qian Liuying, Li Dongxue, Li Fengyan, Wang Peng, Zhao Tianbo
Abstract656)      PDF (4332KB)(474)      
Microcapsules consisting of 58# paraffin wax used as the cores and melamineformaldehyde resin used as the shell were synthesized by the insitu polymerization, and the improvement of apparent morphology and core content of microcapsules was researched. The effects of pH adjustment method, the type of curing agent and stratified treatment on morphology and thermal storage property of microcapsule were studied by SEM, PSDA and DSC. It indicates that pH adjustment is an important factor to microcapsules' morphology and the overall property of microcapsules is greatly improved when NaCl is used as curing agent. After stratified processing, particle sizes of the microcapsules show unimodal distribution and core material content is up to 86.1%.
2016, 29 (3): 7-11. DOI: 10.3969/j.issn.1006-396X.2016.03.002
Effect of Promoters on Performance of CuOZnOZrO2 Catalyst Prepared for CO2 Hydrogenation to Methanol
Li Peipei, Qin Yucai, Li Qiang, Mo Zhousheng, Zhang Yuanyuan, Song Lijuan
Abstract594)      PDF (1940KB)(464)      
CuOZnOZrO2 catalyst was modified by combustion method, using Al2O3, CeO2, NiO metal oxides as promoters. The effects of Al2O3, CeO2, NiO on phase composition and catalyst structure were illuminated by using Xraydiffraction (XRD), temperatureprogrammed reduction ofhydrogen(H2TPR), temperatureprogrammed desorption of hydrogen (H2TPD) and carbon dioxide (CO2TPD) techniques. And the effects of the three chosen promoters on catalytic performance for CO2 hydrogenation to methanol were studied in a fixedbed plug flow reactor. The results indicated that the three promotes of Al2O3, CeO2, NiO all contributed to improving theactivity of catalysts and CeO2modified catalyst had best catalytic performance. Moreover, the three promotes all could inhibit CuO crystal grain growth and improve the dispersion of CuO, which could benefit the reduction of catalysts and H2 adsorptiondissociation. Besides that, the three metal oxides could modulate the intensity amount of basic sites on the catalyst surface in different degrees. Comparing with NiOmodified catalyst, CeO2modified catalyst and Al2O3 modified catalyst both possessed higher basic intensity and more basia sites, which led to CO2 adsorptionactivation easily.
2016, 29 (3): 12-17. DOI: 10.3969/j.issn.1006-396X.2016.03.003
Super Gravity Method of Refinery Dry Gas Selectivity MDEA Desulfurization Experiment Research
Ma Zhiyan
Abstract546)      PDF (2470KB)(463)      
Refinery dry gas contains a lot of hydrogen sulfide and carbon dioxide. In order to improve the dry gas desulfurization efficiency and the effect of the selective absorption desulfurization, in this paper, the super gravity rotating bed equipment was used as absorption desulfurization reactor instead of traditional absorption tower for experimental research. Rotating speed, absorbent dosage and absorption temperature were researched. The optimum operation parameters is: dry gas flow rate of 4 500 m3/h, the condition of pressure of 0.8 MPa, absorbent dosage of 8 m3/h, rotating speed of 800 r/min, absorption temperature of 40~45 ℃. A better absorption effect can be obtained, and hydrogen sulfide content in dry gas can be controlled to 0.01%, which satisfies the requirement of subsequent sulfur emissions. The results have shown that the shorter the retention time in the reactor is, the better the absorbent selectivity of hydrogen sulfide absorption effect is. Rotating bed reactor can replace traditional absorption tower.
2016, 29 (3): 18-22. DOI: 10.3969/j.issn.1006-396X.2016.03.004
Effect of Spontaneous Imbibition on Tight Reservoirs
Pu Yu, Wang Xiuyu, Pu Ling
Abstract706)      PDF (2353KB)(397)      
The tight oil resource is extremely abundant in China, but the production and researches of tight oil is just at the beginning stage. There are great challenges in developping the tight reservoirs. Although small pore size and low permeability can greatly increase the development difficulty, spontaneous imbibition mostly resulted from the capillary pressure is a very important and useful way for tight oil production. In the laboratory experiments through the homemade imbibition apparatus and the effects of different parameters on the imbibition recovery factor was investigated. The results show that the imbibition recovery factor is significantly increased with the increasing of temperature. For rocks with similar parameters ,the recovery factor is increased as the formation water salinity decreases within a certain range. The recovery factor by imbibition varied due to the different boundary conditions. In addition, the curves show good normalization character after processing the data with dimensionless, which can be used to estimate the actual production efficiency of the field. Undoubtedly, the research is of great significance for effectively developing the tight oil reservoir.
2016, 29 (3): 23-27. DOI: 10.3969/j.issn.1006-396X.2016.03.005
Study and Evaluation of ASP Flooding in Daqing Oilfield
Wang Liya, Yang Zhao, Zhou Fu
Abstract626)      PDF (1546KB)(341)      
The field experiment of AlkaliSurfactantPolymer flooding utilizing domestic plant oil carboxylate surfactant firstly on the N block in Daqing oilfield is investigated. Imported sulphonate surfactant used as ASP flooding in Daqing oilfield utilizing is more costly. To reduce cost and increase economic efficiency, plant oil surfactant was firstly employed on the N block in Daqing oilfield. In this experiment, PBH808E carboxylate was used as surface active agent. The test results of asp flooding through indoor core displacement experiment and field experiment were analyzed. It presented that the oil recovery of ASP flooding was more than 20 percent compared with water flooding. Oil emulsification was important to effect oil recovery efficiency. Tracking and adjusting system viscosity can get better trial result. Study and evaluation in this test have a positive effect on the research of ASP flooding in Daqing oilfield.
2016, 29 (3): 28-32. DOI: 10.3969/j.issn.1006-396X.2016.03.006
The Research of Microcosmic Pore Structure Parameters and Oil Driving Efficiency of Ultra Low Permeability Reservoir in Outer Edge of Daqing Oilfield
Yin Daiyin, Lyu Teng, Chen Xinkuang
Abstract515)      PDF (4239KB)(313)      
In order to study the relationship of oildriving efficiency with microcosmic pore structure in the Changyuan ultralow permeability reservoir of outer edge of Daqing oilfield, the CT technology was used to research dozens of natural cores. Lots of data such as pore radius, throat radius, porethroat ratio, coordination numbers, tortuosity and shape factor were obtained. The waterflood experiment was conduct and each oildriving efficiency was recorded, then the effect of pore structure parameter on oildriving efficiency was studied. After the standard processing, the linear regression equation of pore structure parameters and oildriving was obtained. The results showed that, among all the parameters, the average throat radius was the critical element with a factor of 0.531. While the average pore radius was considered to be insignificant with a factor of 0.045.
2016, 29 (3): 33-37. DOI: 10.3969/j.issn.1006-396X.2016.03.007
Research on Performance of Shearing Resistance Sealing Agent DLJ5 Used in Drilling Engineering
Yan Jian, Lyu Haiyan, Li Zhuanhong
Abstract580)      PDF (2043KB)(321)      
Aiming at the poor plugging performance of conventional bridge plug plugging material or the problem of repeat leakage in the drilling process of fractured reservoir, a kind of shearing resistance sealing agent DLJ5 was synthesized by the adding of hectorite. The microstructure of DLJ5 was researched by laser particle size analyzer and diffractometer. The swelling property, shearing resistance property, compatibility with drilling fluid and plugging performance were evaluated through lab tests. The results show that the initial average particle size of sealing agent DLJ5 is 204.5 μm. The internal double network structure with organic and inorganic can improve the strength of sealing agent. The swelling ratio of sealing agent DLJ5 is 35.52 in the simulation formation water of 50 ℃. The sealing agent has good shearing resistance properties and good compatibility with Changqing drilling fluid. The sealing agent also has good plugging property in high salinity reservoir. The shearing resistance sealling agent has broad application prospects in the drilling of fractured reservoir.
2016, 29 (3): 38-42. DOI: 10.3969/j.issn.1006-396X.2016.03.008
Facies Controlled Modeling Technology under Multifactor Control:A Case Study of CⅢ Formation, Tazhong 40 Well Block
She Lingfeng, Ouyang Chuanxiang, Wang Meng
Abstract610)      PDF (5127KB)(435)      
Distribution of sand body in CⅢ Formation Tazhong 40 well block is complicated and reservoir heterogeneity is strong. Taking deterministic modeling and stochastic modeling method into consideration, the structural model, sedimentary microfacies model and attribute model controlled by microfacies of CⅢ Formation Tazhong 40 well block were established by Petrel software in which the sedimentary microfacies model was established under four restrained mechanisms, then the recalculation of the geological reserves was also completed on the basis of the models. Research shows that the microfacies which can store the oil was dominated by highenergy foreshore sandsheet, the porosity and permeability of the third layer were better than that of the first and second layer in research area obviously. What's more, the value of geological reserves calculated by threedimensional geological model was objective and reasonable, which layed the foundation for further development and adjustment of CⅢ Formation Tazhong 40 well block. In general, it owned reference significance for the application of faciescontrolled modeling insimilar area.
2016, 29 (3): 43-47. DOI: 10.3969/j.issn.1006-396X.2016.03.009
Analysis on the Development Effect of High Angle Directional Well in Fault Edge
Wang Chunmei
Abstract463)      PDF (3566KB)(302)      
The remaining oil in the fault edge of Lamadian oilfield is relatively enrichment. Conventional methods cannot accurately describe the fault structure features. Therefore, in this text using the combination of well and seismic technology as the core, multidisciplinary reservoir fine description as method, structural characteristics is studied, the remaining oil is quantified, and the residual oil along fault is tapped by taking the high angle directional well. Since 2009, 12 high angle directional well are successively designed in the 37#, 51# and 15# fault edge, which has made good effects. Through the analysis of high angle directional well development effect, the high angle directional well technology characteristics and the tapping type of potential of residual oil were determined. By optimizing the adjustment measures, the longterm development of high angle directional well was effectively guaranteed. At the same time, the large fault edge remaining potential was further defined, which provide a basis for the development of fault edge and increase of water flooding recoverable reserves.
2016, 29 (3): 48-54. DOI: 10.3969/j.issn.1006-396X.2016.03.010
Surface Wellbore Trajectory Optimization Design for Shale Gas Development in Changning Block
Huo Yang, Zhu Yan
Abstract517)      PDF (1866KB)(312)      
There are many difficulties during the shale gas development and drilling process in Changning block, such as serious nature deviation angle of surface formation, poor drillability, small deviation in anticollision and angle maintaining interval, collapse in the angle descending interval, long drilling period, high drilling cost, and so on. Based on the disadvantages analysis of the previous design plan, the well distribution plan, well trajectory design and drilling technology is further optimized for the cluster wells, and a new trajectory optimization scheme is proposed. The technology scheme has achieved good results through field test. The drilling speed has been improved obviously and the drilling period has been reduced significally, which provide technical support for the shale gas development in Changning block.
2016, 29 (3): 55-58. DOI: 10.3969/j.issn.1006-396X.2016.03.011
Influence Factors of Polymer Flooding Sewage Dilute Polymer Solution Viscosity
Zhang Jihong, Yang Fengyuan
Abstract498)      PDF (1537KB)(296)      
Polymer flooding sewage was used to dilute polymer solution XingBei oilfield. The low viscosity and poor stability made it unable to reach the injection requirement. A series experiments were made to study the problems. The results showed that Fe2+ and Na+ in the polymer flooding sewage were the major causes which reduced viscosity of polymer solution. Suspended solids and bacteria were the secondary factors. In order to effectively use polymer flooding sewage recycle dilute polymer solution and to make the oil field to achieve the purpose of economic and environmental development, the sewage quality was improved by oxygen exposure and putting flocculent. The viscosity of polymer solution was increased by 10.83 mPa·s compared with untreated polymer flooding sewage dilute, and viscosity loss rate was decreased from 28.4% to 12.16%, reaching the reinjection standard.
2016, 29 (3): 59-63. DOI: 10.3969/j.issn.1006-396X.2016.03.012
Development and Performance Evluation on a Crosslinker of Water Shutoff Agent
Zhang Mingfeng, Li Jun
Abstract580)      PDF (1854KB)(392)      
HPAM gel is the most widely used and most effective chemical water shutoff agent at home and abroad. Phenol/formaldehyde is commonly used for crosslinking agent of HPAM gel. However, its high toxicity,especially the carcinogenic,restricts its application severely in the oilfield. In this paper,a lowtoxicity crosslinking agent was synthesized firstly,and then the geation kinetic of HPAM crosslinking with the composite crosslinker was studied,in which THMBPA was the main crosslinking agent and polyethylene polyamine TET as assisting crosslinking agent. The influence of temperature,initial pH,composite crosslinker ratio and salt concentration on the gealtion time and long term stability were investgated. Experimental results showed that the gelation time of the gel system can be arbitrarily adjusted at the range of 10~120 h at 120 ℃,and gel could remain stable for 90 days at 120 ℃ and 100 days at 120 ℃. Long sand packed tube plugging experiments showed that the water shutoff agent had good sealing ability and plugging rate could reach 90.6%.
2016, 29 (3): 64-68. DOI: 10.3969/j.issn.1006-396X.2016.03.013
The Risk Assessment of the Segmented Marine Riser Based on Gray Relevance Theory
Zheng Yunhu, Jiang Feng, Du Chaofei
Abstract458)      PDF (1588KB)(349)      
Each work area of the marine riser has its corresponding specific sea conditions, and the feasibility of macroevaluate is poor. For the feasibility of the whole problem of poor riser assessment, a method was proposed to segment the entire riser calculations, and assessment comprehensively. The marine riser common risk factors were collected to establish risk assessment model, and the gray correlation theory was used to assessment segmented riskof marine riser. According to the major risk factors associated with the risk of occurrence probability, for each segment, the invalidation problem and unreasonable weightswere calculated, the probability of failure of each section of the riser was further calculated by combining the weight with failure correlation coefficient of each section in a variety of major risk factors . This method of risk assessment of the marine riser provides a new way to strengthen the management and maintenance for marine riser of each section.
2016, 29 (3): 69-73. DOI: 10.3969/j.issn.1006-396X.2016.03.014