Salt Cosolvent-Combustion Rapidly Synthesized Small-Size Rod Zinc Oxide

doi:10.3969/j.issn.1006-396X.2012.05.005

Journal of Petrochemical Universities ›› 2012, Vol. 25 ›› Issue (5): 18-21.DOI: 10.3969/j.issn.1006-396X.2012.05.005

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Salt Cosolvent-Combustion Rapidly Synthesized Small-Size Rod Zinc Oxide

1. School of Chemistry & Material, Liaoning Shihua University, Fushun Liaoning 113001, P.R.China； 2.School of Petrochemical Engineering, Liaoning Shihua University, Fushun Liaoning 113001, P.R.China; 3.CNPC Fushun Chemical Plastics Plant, Fushun Liaoning 113005, P.R.China

Received:2012-06-01 Published:2012-10-25 Online:2012-10-25

盐助溶燃烧法快速合成小粒径棒状氧化锌

李秀萍¹,赵荣祥²,刘春生¹,高霄汉¹,冯锦烨³

1.辽宁石油化工大学化学与材料科学学院,辽宁抚顺113001;2.辽宁石油化工大学石油化工学院,辽宁抚顺113001;3.中国石油抚顺石化分公司抚顺化工塑料厂,辽宁抚顺113005

作者简介:李秀萍（１９７５－），辽宁康平县，讲师，在读博士
基金资助:
国家青年基金项目（２１００３０６９）

Abstract

Abstract: With zinc nitrate as the oxidant and ascorbic acid as reducing agent and a new burners, combustion rapidly synthesized milky and rod zinc oxide. The burning agent dose, calcined or not, calcination temperature, adding cosolvent or not were inspected. The experiment show ratio of ascorbic acid and zinc [KG*4]nitrate [KG*4]is [KG*4]3∶1, ratio [KG*4]of [KG*4]ascorbic [KG*4]acid [KG*4]and [KG*4]cosolvent is 1∶ 0.5. Product of combustion wasnt calcined and washed, which is high purity and good crystallinity. The samples more fluffy and shorter by adding cosolvent. The sample was characterized by FTIR, XRD, UV-Vis, SEM. Zinc oxide has strong absorption in UV-Vis and IR wave band，particles size is micron, morphology is short rod.

Key words: Combustion method, Rod, Zinc oxide

摘要： 采用一种新型还原性的燃烧剂抗坏血酸与氧化性的六水合硝酸锌为原料，燃烧法合成乳白色棒状氧化锌，对燃烧剂的用量、是否煅烧和煅烧温度、是否加入助溶剂进行考察。结果表明，燃烧剂与六水合硝酸锌的物质的量之比为3∶1，六水合硝酸锌与助溶剂物质的量之比为1∶0.5，样品不经洗涤和煅烧，其纯度和结晶度较高。加入助溶剂样品更加蓬松，样品棒更短。样品经FTIR, XRD, UV-Vis, SEM表征，结果表明所制备的氧化锌在紫外和红外都有强吸收，粒径可达微米级，形貌为短的棒状。

关键词: 燃烧法 , 棒状 , 氧化锌

LI Xiu-ping,ZHAO Rong-xiang,LIU Chun-sheng,et al. Salt Cosolvent-Combustion Rapidly Synthesized Small-Size Rod Zinc Oxide[J]. Journal of Petrochemical Universities, 2012, 25(5): 18-21.

李秀萍,赵荣祥,刘春生,高霄汉,冯锦烨. 盐助溶燃烧法快速合成小粒径棒状氧化锌[J]. 石油化工高等学校学报, 2012, 25(5): 18-21.

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Salt Cosolvent-Combustion Rapidly Synthesized Small-Size Rod Zinc Oxide

盐助溶燃烧法快速合成小粒径棒状氧化锌

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