关键词: 酸化油, 破乳脱水, 检验方法, 控制指标, 返排液量

Abstract: The flowback fluid during oil acidizing operation process would directly enter the gathering and transportation system,resulting in deterioration or invalidation of conventional treatment agents,such as demulsifiers.The flowback fluids from the Chengdao Oilfield were divided into two types ，one is high mass concentration,the other is low mass concentration.The high mass concentration flowback fluid is transported back by the operating ships to the shore for further treatment,and the low mass concentration flowback fluid is directly discharged into the gathering and transportation system under the ground.The flowback cycle is long and affected by sea conditions. In order to reasonably estimate the amount of high mass concentration flowback fluid produced by crude oil dehydration process,this paper analyzes the factors affecting the oil⁃water separation of acidified flowback fluid.The volume of flowback fluid and indicators of water in two acidified oil wells were monitored,and thermal deposition of mixed flowback fluid and crude oil were tested. According to the demulsification effect and the water content of crude oil form the joint station, the quantified critical control index are listed as: the pH value of the water from the acidified oil well is higher than 6, the iron ion concentration is lower than 250 mg/L；and the auxiliary control index: the amount of backflow reaches 6 times higher than that of the acid liquid. An inspection method is proposed for the on⁃site operation of the flowback fluid discharging into the gathering and transportation system, properly reducing the flowback time without adding a new processing flow, which is beneficial to increase the oil well production rate and improve economic efficiency.

Key words: Acidified oil, Demulsification and dehydr ation, Test method； Control indicators, Flowback fluid volume