Journal of Liaoning Petrochemical University

Journal of Liaoning Petrochemical University ›› 2013, Vol. 33 ›› Issue (3): 16-18.

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Catalytic Synthesis of Butyl Oleate by Using Stannum Silicotungstat

LAI Junling1, LIU Gang2, WANG Jing1, LUO Genxiang1   

  1. 1.School of Chemistry and Materials Science, Liaoning Shihua University, Fushun Liaoning 113001, China; 2.Fushun Shihua Economic And Technical Development Industry General Corporation, Fushun Liaoning 113013, China
  • Received:2012-12-25 Published:2013-09-25 Online:2017-07-14

硅钨酸锡催化合成油酸正丁酯

赖君玲1,刘刚2,王婧1,罗根祥1   

  1. 1.辽宁石油化工大学化学与材料科学学院,辽宁抚顺113001;2.抚顺石化经济技术开发实业总公司,辽宁抚顺113013
  • 作者简介:赖君玲(1976-),女,辽宁大石桥市,副教授,硕士

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Abstract: The catalyst stannum silicotungstat was prepared and characterized, then the esterification of nbutanol and oleic acid was studied. The effect of molar ratio of acid to alcohol, the amount of catalysts, reaction time and reaction temperature were investigated. Under the optimum conditions, the conversion ratio of oleic acid is 90.4%.

Key words: Stannum silicotungstat , Butyl oleate , Esterification　

摘要： 合成出硅钨酸锡催化剂,进行了XRD和TG的表征并用于油酸和正丁醇的酯化反应。考察了酸醇物
质的量比、催化剂与油酸的质量比、反应时间和反应温度对酯化反应的影响。在最佳实验条件下,油酸的转化率最
高为90.4%。

关键词: 硅钨酸锡 , 油酸正丁酯 , 酯化反应

Cite this article

LAI Junling, LIU Gang, WANG Jing, LUO Genxiang. Catalytic Synthesis of Butyl Oleate by Using Stannum Silicotungstat[J]. Journal of Liaoning Petrochemical University, 2013, 33(3): 16-18.

赖君玲,刘刚,王婧,罗根祥. 硅钨酸锡催化合成油酸正丁酯[J]. 辽宁石油化工大学学报, 2013, 33(3): 16-18.

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