Determination of Copper and Iron in Walnut Oil by MPT - AES

Journal of Liaoning Petrochemical University ›› 2007, Vol. 27 ›› Issue (1): 21-23.

Previous Articles Next Articles

Determination of Copper and Iron in Walnut Oil by MPT - AES

School of Petrochemical Technology , Liaoning University o f Petroleum & Chemical Technology ,Fushun Liaoning 113001 , P. R. China

Received:2006-10-25 Published:2007-03-20 Online:2017-07-05

MPT - AES 法测定核桃油中铜和铁

邵　海, 宫晓杰, 李丽华, 张金生

辽宁石油化工大学石油化工学院, 辽宁抚顺113001

作者简介:邵海(1980 - ), 男, 浙江镇海县, 硕士。

Abstract

Abstract:

　 The analytical methods for copper and iron element in walnut oil were studied by microwave plasma torch atomic emission spectrometry (MPT - AES) using microwave plasma torch (MPT) as excitation light source , argon as supporting gas , and peneumatic nebulization sampling system. Some experimental parameters (including microwave power , carrier gas flow rate , supporting gas flow rate , oxygen shied gas flow rate , effect of acid, coexistence ions) were investigated and optimized. The linear range s o f copper and iron is 0. 05 ～ 100, 0. 1～ 100μg /m L, respectively . The detection limits is 5. 3, 22. 1ng /m L, respectively . The recoveries are both in the range of 96. 4 %～ 102. 2% and the RSD of the method is less than 3. 2%.

null

Key words: 　Microwave extraction , , Microwave coupled plasma , , Atomic emission spectrometry , , Walnut oil , , Copper , , Iron

摘要：

　用微波等离子炬(MPT)作激发光源, 氩气为载气, 用气动雾化进样, 研究了微波等离子体炬原子发射光谱法(MPT - AES)测定核桃油中铜和铁元素。考察并优化了微波功率、工作气流量、载气流量、氧屏蔽气流量、酸效应、共存离子等实验参数。测定铜和铁的检出线分别为5. 3 , 22. 1 ng / mL 。RSD均小于3. 2 %, 线性范围分别为0. 05～ 100 , 0. 1 ～ 100μg /m L, 加标回收率均在96. 4 %～ 102. 2 %。

关键词: 微波萃取, 　微波等离子体炬, 　原子发射光谱法, , 核桃油, 　铜, 　铁

CLC Number:

null

SHAO Hai,GONG Xiao - jie,LI Li - hua,ZHANG Jin - sheng. Determination of Copper and Iron in Walnut Oil by MPT - AES[J]. Journal of Liaoning Petrochemical University, 2007, 27(1): 21-23.

邵　海, 宫晓杰, 李丽华, 张金生. MPT - AES 法测定核桃油中铜和铁[J]. 辽宁石油化工大学学报, 2007, 27(1): 21-23.

[1]	Lei GUAN, Bowen FAN, Ying WANG, Xin WANG. Synthesis, Crystal Structure and Fluorescence Property of a Copper Coordination Complex with N⁃Donor Ligand [J]. Journal of Liaoning Petrochemical University, 2023, 43(5): 29-33.
[2]	Chun Kang, Huiqiang Ma, Shuang Li. Fe⁃Doped g⁃C₃N₄ Photocatalytic Activation of Persulfate for Degradation of Azo Dyes [J]. Journal of Liaoning Petrochemical University, 2022, 42(5): 13-17.
[3]	Yichen Li, Fei Xie, Jian Li, Xiaolong Zhang, Yang Zhao, Yuguo Wu. Study of Corrosion Behavior of X52 Steel in Marine Environment [J]. Journal of Liaoning Petrochemical University, 2022, 42(5): 26-31.
[4]	Xiaoxue Mu, Wei Ding, Xiaofan Zhang, Yongchuan Dai, Zhongxing Geng, Yu Li. Preparation and Characterization of Iron Modified MoNi/γ⁃Al₂O₃ Catalysts [J]. Journal of Liaoning Petrochemical University, 2022, 42(4): 6-10.
[5]	Guohua Diao, Liwei Pan, Lin Fan, Xinyu Han, Hexiang Zhong. Review of Copper⁃Based Catalysts for Electrocatalytic Reduction of Carbon Dioxide [J]. Journal of Liaoning Petrochemical University, 2021, 41(4): 1-8.
[6]	Yuke Liu, Fei Yan, Jing Sun, Mingdong Zhou. Copper⁃Catalyzed Synthesis of a Long Alkyl Branched Fatty Alcohol [J]. Journal of Liaoning Petrochemical University, 2021, 41(4): 17-21.
[7]	Chen Yu, Yang Jiang, Zhao Xiaolong, Li Shengke. Environmental Friendly Oil Sludge Treatment Agent for Petrochemical Wastewater [J]. Journal of Liaoning Petrochemical University, 2020, 40(4): 1-4.
[8]	Sun Cai， Gao Ying， Zhang Jing. Recent Advancement of Iron Oxide Photoelectrocatalytic Materials [J]. Journal of Liaoning Petrochemical University, 2020, 40(2): 30-37.
[9]	Li Zhenya, Liu Zhibo, Yu Fang. Study on the Technology of Diamine Monoprotection [J]. Journal of Liaoning Petrochemical University, 2020, 40(1): 32-34.
[10]	Zhou Jie，Zhang Fenghua，Ding Xiaoguang，Yu Fang. CuCl⁃Promoted C-O Cross Coupling of p⁃Methyl Bromobenzene and Phenol [J]. Journal of Liaoning Petrochemical University, 2019, 39(5): 21-25.
[11]	Jia Hongyu， Liu Ningning, Zhang Zhe, Yin Yunzhi. Research Progress of Poly(Lactic Acid) Separation Membrane [J]. Journal of Liaoning Petrochemical University, 2018, 38(1): 1-9.
[12]	Zhang Huan，Li Qingdong. Analysis of the Relationship between Environmental Pollution and Economic Development under the New Normal [J]. Journal of Liaoning Petrochemical University, 2018, 38(05): 89-94.
[13]	Kong Lingsen， Wu Ming， Jia Fengrui， Liu Guangxin， Yang Yujie， Yue Qiang. Optimized Water-Consumption Network in Refinery Enterprises and Its Evaluation Index System [J]. Journal of Liaoning Petrochemical University, 2018, 38(04): 15-20.
[14]	. Removal of Sulfides from Simulated Oil by CH₃CONH₂/ZnCl₂ Deep Eutectic Solvent [J]. Journal of Liaoning Petrochemical University, 2017, 37(5): 1-7.
[15]	LiuYujuan,XuJi,TongYufei,et al. Progress in Research of the Synthesis Methods of Nanometer Ceria [J]. Journal of Liaoning Petrochemical University, 2017, 37(5): 8-12.

Determination of Copper and Iron in Walnut Oil by MPT - AES

MPT - AES 法测定核桃油中铜和铁

PDF

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics